HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl phosphite → HCID 53885870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Reactant | 1-(Bromomethyl)-4-nitronaphthalene | HCID 12749163 | — |
| Product | HCID 53885870 | HCID 53885870 | — |
Reaction Steps
1-Bromomethyl-4-nitronaphthalene and trimethylphosphite ((CH3O)3P) were treated in the same manner as in Reference Example 43 to yield dimethyl (4-nitro-1-naphthyl)methylphosphonate, which was then recrystallized from ethanol-hexane to yield yellow prisms having a melting point of 128°-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716944 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-b8425a12ef6b4ac98801c5658e1cbdb9 |
| Source note | uspto-grants-1998_02 |