HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15284565, compound → HCID 19701073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15284565 | HCID 15284565 | — |
| Reactant | 1,1-Dimethyl-2-(2-methylprop-2-en-1-ylidene)hydrazine | HCID 54237122 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19701073 | HCID 19701073 | 53.4% |
Reaction Steps
Methacrolein dimethylhydrazone (90 mg, 0.75 mmol) in one portion was added to a solution of 3-phenyl-5,8-dimethoxy-2-(1H)-quinolinone (190 mg, 0.71 mmol) in chloroform (50 ml.) The solution was agitated at room temperature for 3 hours and was evaporated. The residue was chromatographed over silica gel, eluting with ethyl acetate to give 120 mg (50%) of 6-methyl-3-phenyl-1H-1,8-diazaanthracen-2,9,10-trione (I-j). m.p. 275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716963 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-a49a1312e45e4bd88ca68ad2eb82c618 |
| Source note | uspto-grants-1998_02 |