N-bromobutanimide → HCID 19701418, compound

HRID 861989Notes

Reaction equation

HRID 861989 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N:9]2[C:17](=[O:18])[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[C:10]2=[O:19])=[N:6][C:7]=1[CH3:8].C1C(=O)N([Br:27])C(=O)C1>C(Cl)Cl>[Br:27][CH2:8][C:7]1[N:6]=[C:5]([N:9]2[C:10](=[O:19])[C:11]3[C:16](=[CH:15][CH:14]=[CH:13][CH:12]=3)[C:17]2=[O:18])[CH:4]=[CH:3][C:2]=1[Cl:1]

Participants

4

Reactant 2

HCID 67184N-bromobutanimideHCID 19701489HCID 19701489, compound

Product 1

HCID 19701418HCID 19701418, compoundYield 116.1%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Following the procedure of Example 2, the product from Example 25 (6.07 g, 22 mmol) was reacted with NBS (3.96 g, 22 mmol) in CH2Cl2 (150 mL). The crude title product (8.98 g, >100%) was obtained and used without further purification.

Sources & evidence

ORD record
ord-31095e4edf8b452493862a65e338e3a6
Source dataset
uspto-grants-1998_02
Patent number
US05716964

Reaction notes

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