化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Diphenylethylamine → N-(1,2-Diphenylethyl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Diphenylethylamine | HCID 26482 | — |
| 反応物 | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| 生成物 | N-(1,2-Diphenylethyl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 15380259 | — |
反応手順
A procedure similar to that described in Example 3(b) was repeated, except that S-2-pyridyl 3-cyanoandrosta-3,5-diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 1,2-diphenylethylamine were employed as starting materials, in relative proportions similar to those used in that Example, to give the title compound in a quantitative yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05717088 |
| 出典データセット | uspto-grants-1998_02 |
| ORD ID | ord-cf4dcbbb356b498ab5909dd42de7701b |
| 出典メモ | uspto-grants-1998_02 |