化工社化工社 化学情報印刷レポート · 研究参考用
Tert-Butylamine → 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tert-Butylamine | HCID 6385 | — |
| 反応物 | 3-Cyanoandrosta-3,5-diene-17beta-carboxylic acid | HCID 15380254 | — |
| 生成物 | 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide | HCID 67646951 | 81% |
反応手順
Following a procedure similar to that described in Preparation 16a, but using 3-cyanoandrosta-3,5-diene-17β-carboxylic acid [prepared as described in Example 1(b)] and t-butylamine as starting materials, in relative proportions similar to those used in that Preparation, the title compound was obtained in a yield of 81%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05717088 |
| 出典データセット | uspto-grants-1998_02 |
| ORD ID | ord-0dbbd67c48fd4b9db0ae66e1af54153b |
| 出典メモ | uspto-grants-1998_02 |