HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chromanone → Chroman-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chromanone | HCID 68110 | — |
| Reactant | HCID 178418435 | HCID 178418435 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Chroman-4-ol | HCID 92890 | — |
Reaction Steps
The compound 3 is reduced using a reducing agent such as sodium boron hydride in a solvent such as methanol, ethanol and tetrahydrofuran, preferably in an alcohol solvent such as methanol and ethanol, under cooling to room temperature to give 4-chromanol (compound 4 wherein R1, R2 and R3 are as defined above).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719155 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-5a718ffded6043de9fbf0c80a61f7652 |
| Source note | uspto-grants-1998_02 |