HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → 2-Nitro-5-(2-propyloxy)benzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | 3-(Hydroxymethyl)-4-nitrophenol | HCID 108946 | — |
| Product | 2-Nitro-5-(2-propyloxy)benzyl alcohol | HCID 54487340 | — |
Reaction Steps
10 g (60 mmol) of 5-hydroxy-2-nitrobenzyl alcohol were reacted with 7.0 ml (70 mmol) of isopropyl iodide analogously to Example 4a); after purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719164 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-b7f99e2042554d2789c4539143f2549a |
| Source note | uspto-grants-1998_02 |