참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 4-Octanoylphenethyl acetate | HCID 21707528 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 2-Pentadecyn-1-ol | HCID 534429 | — |
반응 단계
The compound (12,374 g) of (1) above was dissolved in a N solution (230 ml) of hydrochloric acid in methanol and the mixture was heated at 65° C. for 1.5 hours. The reaction mixture was concentrated under reduced pressure and the residue was purified by silica gel column chromatography to give 8.465 g of 2-pentadecynyl alcohol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05719176 |
|---|
| 출처 데이터셋 | uspto-grants-1998_02 |
|---|
| ORD ID | ord-24ce47e28e2b4af28aaaa5194e344c9f |
|---|
| 출처 메모 | uspto-grants-1998_02 |
|---|
