HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 2-Amino-2-(1,2-dihydroxy-4-octadecenyl)-1,3-propanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 53930981 | HCID 53930981 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Amino-2-(1,2-dihydroxy-4-octadecenyl)-1,3-propanediol | HCID 53863801 | — |
Reaction Steps
A lactone compound (978 mg) of 2-amino-3-hydroxy-2-(1,2-dihydroxy-4-octadecenyl)propionic acid and 403 mg of lithium aluminum hydride were reacted in 33 ml of dry tetrahydrofuran according to the method of Example 274 to give 222 mg of the subject compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719176 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-2b7c9da5aabf4c02a4055671e0c0ede2 |
| Source note | uspto-grants-1998_02 |