Acetic Anhydride → HCID 19699328, compound

HRID 863097Notes

Reaction equation

HRID 863097 reaction equation
[NH2:1][N:2]1[CH:6]=[N:5][N:4]([CH:7]2[CH2:16][CH2:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[CH2:8]2)[C:3]1=[S:17].[C:18](OC(=O)C)(=[O:20])[CH3:19]>>[CH2:8]1[C:9]2[C:14](=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH2:15][CH2:16][CH:7]1[N:4]1[C:3](=[S:17])[N:2]([NH:1][C:18](=[O:20])[CH3:19])[CH:6]=[N:5]1

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 19699360HCID 19699360, compound

Product 1

HCID 19699328HCID 19699328, compound

Procedure

substituting 4-amino-2-(1,2,3,4-tetrahydronaphthalen-2-yl)-2,4-dihydro[1,2,4]triazole-3-thione and acetic anhydride gave N-[1-(1,2,3,4-tetrahydronaphthalen-2-yl)-5-thioxo-4,5-dihydro-1H-[1,2,4]triazol-4-yl]acetamide, m.p. 199°-201° C.

Sources & evidence

ORD record
ord-bc17cf78bda04e8a9ac6b468ff6ba8a8
Source dataset
uspto-grants-1998_02
Patent number
US05719280

Reaction notes

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