HCID 19697793, compound → HCID 19697827, compound

HRID 863262Notes

Reaction equation

HRID 863262 reaction equation
[CH3:1][NH:2][C:3]([C:5]1[CH:14]=[N:13][C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[N:6]=1)=[O:4].C(NC(=O)[C@H](C)C[C@H](O)[C@@H](NC(OC(C)(C)C)=O)CC(C)(C)CC(N1C2C(=CC=CC=2)CCC1C(OC)=O)=O)CCC>C(O)C.[Pd]>[CH3:1][NH:2][C:3]([CH:5]1[CH2:14][NH:13][C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[NH:6]1)=[O:4]

Participants

5

Reactant 2

HCID 19697793HCID 19697793, compoundHCID 131720518HCID 131720518, compound

Product 1

HCID 19697827HCID 19697827, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

0.33 g of 2-(methylaminocarbonyl)quinoxaline in 15 ml of ethanol is hydrogenated in the presence of 0.07 g of palladium-on-charcoal (10% of Pd) at room temperature for 6 h: Rf (P)=0.45.

Sources & evidence

ORD record
ord-2851d428d917455cb9e981c4d65bf87e
Source dataset
uspto-grants-1998_02
Patent number
US05719141

Reaction notes

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