HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl chloroformate → 3(R,S)-Allyloxycarbonylamino-1,2,3,4-tetrahydroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl chloroformate | HCID 18052 | — |
| Reactant | 1,2,3,4-Tetrahydroquinolin-3-amine | HCID 4055118 | — |
| Reactant | 5(S)-tert-butoxycarbonylamino-4(S)-hydroxy-2(R),7,7-trimethyl-8-[3(R,S)-cyclopropylcarbonylamino-1,2,3,4-tetrahydroquinolin-1-ylcarbonyl]-octanoic acid (N-butyl)amide | HCID 131720527 | — |
| Product | 3(R,S)-Allyloxycarbonylamino-1,2,3,4-tetrahydroquinoline | HCID 19697548 | — |
Reaction Steps
In a manner analogous to that described in Example 109b) from 1.0 g of 1.0 g of 3(R,S)-amino-1,2,3,4-tetrahydroquinoline and 0.75 ml of allylchloroformate: Rf (P)=0.81; MS: M+ =232.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719141 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-86f8d821755b4e6b9fbe16052b787399 |
| Source note | uspto-grants-1998_02 |