HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxyquinoline → HCID 19697839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxyquinoline | HCID 11376 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19697839 | HCID 19697839 | — |
Reaction Steps
0.98 ml of methyl isocyanate is added to a suspension of 1.0 g of 3-hydroxyquinoline in 8 ml of methylene chloride and the reaction mixture is heated under reflux for 5 h. Purification by chromatography over 50 g silica gel (mobile phase J) gives 3-(methylaminocarbonyloxy)quinoline as a solid: Rf (L)=0.26.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719141 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-e57fda3ec8e740f5855fde716232c8df |
| Source note | uspto-grants-1998_02 |