HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzyloxycarbonyl-3(R,S)-(1-methoxyethen-2-yl)-1,2,3,4-tetrahydroquinoline → 3(R,S)-methoxyethyl-1,2,3,4-tetrahydroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzyloxycarbonyl-3(R,S)-(1-methoxyethen-2-yl)-1,2,3,4-tetrahydroquinoline | HCID 57219624 | — |
| Reactant | 5(S)-tert-butoxycarbonylamino-4(S)-hydroxy-2(R),7,7-trimethyl-8-[3(R,S)-allyloxymethyl-1,2,3,4-tetrahydroquinolin-1-ylcarbonyl]-octanoic acid (N-butyl)amide | HCID 131720529 | — |
| Product | 3(R,S)-methoxyethyl-1,2,3,4-tetrahydroquinoline | HCID 19697855 | — |
Reaction Steps
The title compound is prepared in a manner analogous to that described in Example 1r) starting from 2.3 g of N-benzyloxycarbonyl-3(R,S)-(1-methoxyethen-2-yl)-1,2,3,4-tetrahydroquinoline: Rf (A)=0.40; FAB-MS: (M+H)+ =192.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719141 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-84caebe73222428a8ddde0e921350704 |
| Source note | uspto-grants-1998_02 |