HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 53986712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 53724777 | HCID 53724777 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53986712 | HCID 53986712 | — |
Reaction Steps
3.5 g (20 mmol) of 2-acetyl-6-(1-propenyl)phenol and 2.1 g (20 mmol) of benzaldehyde are dissolved in 20 ml of ethanol, 4 ml of concentrated NaOH are added, the mixture is stirred overnight, the red crystal slurry is diluted with methanol and acidified with concentrated HCl and, after cooling, the product is filtered off with suction. Orange-red crystals of melting point 95°-98° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721248 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-34730f1132b042fd90648f565f91ad0c |
| Source note | uspto-grants-1998_02 |