Sodium Hydroxide → HCID 19430425, compound

HRID 863453Notes

Reaction equation

HRID 863453 reaction equation
C([O:4][CH2:5][C:6]1[C:14]2[C:13]([Br:15])=[C:12]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[S:11][C:10]=2[CH:9]=[CH:8][CH:7]=1)(=O)C.[OH-].[Na+]>C(O)C>[Br:15][C:13]1[C:14]2[C:6]([CH2:5][OH:4])=[CH:7][CH:8]=[CH:9][C:10]=2[S:11][C:12]=1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 19430426HCID 19430426, compound

Product 1

HCID 19430425HCID 19430425, compoundYield 101.9%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Hydrolysis of the compound from Example XV (1 g) in 100 ml of ethanol with 20 ml of 1N NaOH at room temperature gives, after 2 hours, 0.9 g of the title compound.

Workup

  1. customgives, after 2 hours

Sources & evidence

ORD record
ord-e338265193a7454ab80a71753be5ef85
Source dataset
uspto-grants-1998_02
Patent number
US05721248

Reaction notes

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