HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 19696485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | (3-bromoprop-1-en-2-yl)benzene | HCID 234998 | — |
| Reactant | 3-Hydroxy-2-iodobenzaldehyde | HCID 11459296 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19696485 | HCID 19696485 | — |
Reaction Steps
6.72 g (0.28 mmol) of sodium hydride are dissolved in 660 ml of ether and 120 ml of dimethylformamide under argon, and 64.1 g (0.26 mol) of 3-hydroxy-2-iodobenzaldehyde in 65 ml of ether are slowly added. After the mixture has been stirred at room temperature for 15 minutes, 61 g (0.28 mol) of 3-bromo-2-phenyl-1-propene, dissolved in 60 ml of ether, are added dropwise and the mixture is stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721248 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-cc680a36619f4f3db312da1b344442f9 |
| Source note | uspto-grants-1998_02 |