HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Nitrophenyl)acetic acid → Benzeneacetyl chloride, 4-nitro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Nitrophenyl)acetic acid | HCID 4661 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Benzeneacetyl chloride, 4-nitro- | HCID 6452210 | 100% |
Reaction Steps
A stirred mixture of 4-nitrophenylacetic acid (25 g, 0.138 mol) in thionyl chloride (50 ml, 0.685 mol) was heated at reflux for 2 hours then concentrated to yield 4-nitrophenylacetyl chloride (27.55 g) as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721247 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-cdd0f989aed84df599d7a26af99cf41d |
| Source note | uspto-grants-1998_02 |