HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propenoic acid, 3-phenyl- → 1-Indanone, 3-phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 1-Indanone, 3-phenyl- | HCID 98146 | 85.4% |
Reaction Steps
To 25.0 g of aluminum chloride, 8.5 g of cinnamic acid and 37.5 ml of benzene were added and the mixture was reacted under reflux for 5 hours. The reaction solution was processed by a usual method to obtain 5.1 g of 3-phenyl-1-indanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721288 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-a49f611610274bb892e899afe57aaf15 |
| Source note | uspto-grants-1998_02 |