HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyldimethylsilyl chloride → HCID 54479352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | HCID 10923331 | HCID 10923331 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 54479352 | HCID 54479352 | — |
Reaction Steps
A process according to claim 1, in which (3S,4S)-4-acetoxy-3-phenylacetamido-azetidin-2-one is treated with tert-butyldimethyl chlorosilane in the presence of 4-dimethylaminopyridine in an organic solvent and the (3S,4S)-4-acetoxy-3-phenylacetamido-1-tert-butyldi methylsilyl-azetidin-2-one (III) is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721360 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-cc24fb2c7e5c4902a88e8c293c3406b7 |
| Source note | uspto-grants-1998_02 |