HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octanoyl chloride → N-methyl-N-octanoylacrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Reactant | N-methyl-N-trimethylsilylacrylamide | HCID 19419944 | — |
| Product | N-methyl-N-octanoylacrylamide | HCID 19419945 | — |
Reaction Steps
To 4.1 g (0.0252 mole) of N-methyl-N-trimethylsilylacrylamide was added dropwise 3.66 g of octanoyl chloride at 0° C. After the addition was completed, the mixture was allowed to stir for 45 minutes at room temperature. Complete conversion was indicated by IR after 2 hours and 45 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05560749 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-771719b9f8af41a1afbbfe3892dc5045 |
| Source note | uspto-grants-1996_10 |