2-chloro-N,N-dimethylacetamide → HCID 86749873, compound

HRID 863722Notes

Reaction equation

[NH2:1][C:2]([NH2:4])=[S:3].[Cl:5][CH2:6][C:7]([N:9]([CH3:11])[CH3:10])=[O:8]>>[Cl-:5].[CH3:10][N:9]([CH3:11])[C:7]([CH2:6][S:3][C:2]([NH2:4])=[NH2+:1])=[O:8]

Participants

Reactant 2

HCID 758862-chloro-N,N-dimethylacetamide

HCID 2723790Thiourea

Product 1

HCID 86749873HCID 86749873, compoundYield 89%

Procedure

Example 1 was repeated with thiourea and 2-chloro-N,N-dimethylacetamide, affording the title compound ina yield of 89%.

Sources & evidence

ORD record: ord-c7c98a492acb42b796c04b2ea52bf974
Source dataset: uspto-grants-1996_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05560814

Reaction notes

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