2-Pentanone, 5-chloro- → HCID 86749874, compound

HRID 863723Notes

Reaction equation

[NH2:1][C:2]([NH2:4])=[S:3].[CH3:5][C:6]([CH2:8][CH2:9][CH2:10][Cl:11])=[O:7]>>[Cl-:11].[O:7]=[C:6]([CH3:5])[CH2:8][CH2:9][CH2:10][S:3][C:2]([NH2:4])=[NH2+:1]

Participants

Reactant 2

HCID 799932-Pentanone, 5-chloro-

HCID 2723790Thiourea

Product 1

HCID 86749874HCID 86749874, compoundYield 71%

Procedure

Example 1 was repeated with thiourea and 3-chloropropyl methyl ketone, affording the title compound in a yield of 71%.

Sources & evidence

ORD record: ord-5a055cebef114a808df0d3e09eb9db91
Source dataset: uspto-grants-1996_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05560814

Reaction notes

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