HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium dicyanamide → HCID 131719589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium dicyanamide | HCID 4350929 | — |
| Reactant | HCID 67768813 | HCID 67768813 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 131719589 | HCID 131719589 | 57% |
Reaction Steps
To a stirred solution of Example 3 Part D compound (220 mg, 0.40 mmol) in 3.0 mL of n-BuOH was added sodium dicyanamide (99.0 mg, 1.00 mmol). The reaction mixture was heated to reflux for 14 h and concentrated in vacuo. This was purified by preparative HPLC to give 124 mg (57%) of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05561146 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-adcbe45d1c3e4a778b6055fb9200d9e0 |
| Source note | uspto-grants-1996_10 |