HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → Benzene, 1,3-bis(1-phenylethenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Isoprene | HCID 6557 | — |
| Reactant | Pentamethyldiethylenetriamine | HCID 18196 | — |
| Reactant | 1,3-Diisopropenylbenzene | HCID 77353 | — |
| Reactant | CID 53628100 | HCID 178418400 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzene, 1,3-bis(1-phenylethenyl)- | HCID 118622 | — |
Reaction Steps
Isoprene, sec-BuLi solution (1.3M in cyclohexane), anhydrous tetrahydrofuran (THF), anhydrous dimethylsulfoxide (DMSO), pentamethyldiethylenetriamine (PMDETA) and 1,3-diisopropenylbenzene (1) were obtained from Aldrich Chemical Company, Milwaukee, Wis. 1,3-bis(1-phenylethenyl)benzene (3) was obtained from the Dow Chemical Company, Midland, Mich.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05561210 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-592ca8bafb7d45659bb753cf662c6d1a |
| Source note | uspto-grants-1996_10 |