Acetone → HCID 19417504, compound

Participants

Reaction Steps

Under a nitrogen atmosphere, a solution of 2.8 grams (0.010 mole) of 3-(5-cyclohexylpentyl)aniline hydrochloride and 0.9 gram (0.011 mole) of cyanoguanidine in 100 mL of acetone was stirred at ambient temperature for about four days. After this time, the reaction mixture was filtered to collect a solid. The solid was recrystallized from methanol/diethyl ether and then from water, yielding 2.7 grams of 1-[3-(5-cyclohexylpentyl)phenyl]-2,4-diamino-6,6- dimethyl-1,6-dihydro-1,3,5-triazine hydrochloride, mp 188°-190° C. The NMR spectrum was consistent with the proposed structure.

Provenance & Evidence