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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 865221Generated: November 1, 2026

Methyl iodide → 3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-1,6-dimethylpyridinium iodide

https://huagongshe.com/reaction/865221

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
Reactant3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-6-methylpyridineHCID 19075369—
SolventAcetoneHCID 180—
Product3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-1,6-dimethylpyridinium iodideHCID 19075328—

Reaction Steps

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-hexylthio-1,2,5-thiadiazol-4-yl)-6-methylpyridine (4 mmol) in acetone (5 ml) and the reaction mixture was stirred at room temperature for 20 h. Evaporation of the reaction mixture gave the crude product, which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05565475
Source datasetuspto-grants-1996_10
ORD IDord-4b701e2c85284088a03b6f7fc087a4c6
Source noteuspto-grants-1996_10