HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanol, 3-chloro-2,2-dimethyl- → 1-(Tert-butoxy)-3-chloro-2,2-dimethylpropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanol, 3-chloro-2,2-dimethyl- | HCID 83407 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | 1-(Tert-butoxy)-3-chloro-2,2-dimethylpropane | HCID 15183227 | 78.06% |
Reaction Steps
B.P.=169.0°-174.0° C. GC assay=2.98% cyclohexane, 16.79% 3-chloro-2,2-dimethyl-1-propanol, 78.06% desired product, and 1.17% unknowns.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05567774 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-320d28cab2184754844c1852aa7e16b9 |
| Source note | uspto-grants-1996_10 |