Potassium Hydroxide → HCID 70619391, compound

HRID 866381Notes

Reaction equation

HRID 866381 reaction equation
[C:1]([C:4]1[CH:17]=[CH:16][C:7]([O:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)([OH:3])=[O:2].[OH-].[K+].[K:20]>O>[C:1]([C:4]1[CH:17]=[CH:16][C:7]([O:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)([OH:3])=[O:2].[K:20]

Participants

5

Reactant 3

HCID 14797Potassium HydroxideHCID 738804-(Benzyloxy)benzoic acidHCID 5462222Potassium

Product 1

HCID 70619391HCID 70619391, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A mixture of 4-carboxyphenoxy phenyl methane (5.7g.; 0.025 mole) and potassium hydroxide (1.4g.; 0.025 mole) in water (40ml) were heated at reflux for 1 hr., on cooling the potassium salt was filtered off and dried, m.p. > 340°.

Workup

  1. temperaturewere heated
  2. temperatureat reflux for 1 hr
  3. filtrationwas filtered off
  4. customdried

Sources & evidence

ORD record
ord-4a72ca3767d346b58ce39dde73a6645f
Source dataset
uspto-grants-1978_07
Patent number
US04098816

Reaction notes

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