HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-(Benzyloxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Benzyl p-tolyl ether | HCID 70036 | — |
| Solvent | Sodium Dichromate | HCID 25408 | — |
| Product | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
Reaction Steps
A mixture of 4-methylphenoxy phenyl methane (2g) was suspended in aqueous sodium dichromate solution (20ml. 50%) and concentrated sulphuric acid (10ml) added dropwise with stirring. The mixture was stirred at room temperature overnight then warmed on a water bath for 1hr. The mixture was cooled, diluted with water and the 4-carboxyphenoxy phenyl methane (m.p. 188°) isolated with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04098816 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-ae4c4a93c7aa4cb593dbf89f125d6d34 |
| Source note | uspto-grants-1978_07 |