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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 866407Generated: October 25, 2026

Nicotinic Acid → 2,4-Bis(nicotinamido)-6-phenyl-s-triazine

https://huagongshe.com/reaction/866407

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNicotinic AcidHCID 938—
ReactantBenzoguanamineHCID 7064—
ReactantChloroethyl carbonateHCID 22631361—
SolventPyridineHCID 1049—
Product2,4-Bis(nicotinamido)-6-phenyl-s-triazineHCID 2032103564.5%

Reaction Conditions

Temperature60 °C

Reaction Steps

1.9 g of benzoguanamine and 2.6 g of nicotinic acid are dissolved in 50 ml of pyridine and mixed with 2.2 g of chloroethyl carbonate. After heating the mixture at 60° C with agitation for 3 hours, it is processed as described in Example 4 to yield 1.3 g of 2,4-bis(nicotinamido)-6-phenyl-s-triazine [dinicotinoylbenzoguanamine].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04098892
Source datasetuspto-grants-1978_07
ORD IDord-0822b237088c43928d4831dd80ae9313
Source noteuspto-grants-1978_07