Ethylenediamine → HCID 178433308, compound

HRID 866422Notes

Reaction equation

HRID 866422 reaction equation
[C:1]([NH:3][C:4](=[N:7][CH2:8][CH2:9][S:10][CH2:11][C:12]1[NH:16][CH:15]=[N:14][C:13]=1[CH3:17])SC)#[N:2].[CH2:18]([NH2:21])[CH2:19][NH2:20]>>[C:1]([NH:3][C:4]([NH:20][CH2:19][CH2:18][NH2:21])=[N:7][CH2:8][CH2:9][S:10][CH2:11][C:12]1[NH:16][CH:15]=[N:14][C:13]=1[CH3:17])#[N:2]

Participants

3

Reactant 2

HCID 3301EthylenediamineHCID 178503877HCID 178503877, compound

Product 1

HCID 178433308HCID 178433308, compound

Procedure

Reaction of N-cyano-N'-[2-((4-methyl-5-imidazolyl)methylthio)-ethyl]-S-methylisothiourea with excess ethylenediamine at room temperature afforded the title compound m.p. 164°-167° (from acetonitrile-ethanol). (Found: C, 46.9; H, 6.5; N, 35.1; S, 11.1% C11H19N7S requires: C, 47.0; H, 6.8; N, 34.8; S, 11.4%).

Sources & evidence

ORD record
ord-059a56fac5aa4305a6a82021ba65cef0
Source dataset
uspto-grants-1978_07
Patent number
US04098898

Reaction notes

Loading…