Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → 2,5-Dimethyl-3-[(3-methylbutyl)disulfanyl]furan
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Isoamyl mercaptan | HCID 10925 | — |
| 반응물 | 2,5-Dimethyl-3-furanthiol | HCID 41569 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 2,5-Dimethyl-3-[(3-methylbutyl)disulfanyl]furan | HCID 71398367 | — |
반응 단계
0.64 Grams (0.005 moles) of 2,5-dimethyl-3-furanthiol and 1.04 grams (0.01 moles) of isoamyl mercaptan are dissolved in 12 ml anhydrous diethyl ether. 0.8 Grams (0.0075 moles) of sodium carbonate dissolved in 8 ml water is added with stirring to the reaction mass. 1.9 Grams (0.0075 moles) of iodine dissolved in 6 ml anhydrous diethyl ether is then added dropwise to the reaction mass until the iodine color remains. The reaction mass is then stirred for a period of 30 minutes.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04098910 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-3011bd594a574374a819b8ec8fd598d9 |
| 출처 메모 | uspto-grants-1978_07 |