HCID 70619294, compound → HCID 20286840, compound

Participants

Reaction Steps

2.5 g (6.5 mmols) of 3,12-dicyclooctyl-1,2-diaza-1,5,9-cyclododecatriene are hydrogenated, in 100 ml of cyclohexane in a stirred autoclave and with the addition of 0.6 g of rhodium-aluminum oxide (5% by weight of rhodium), first at room temperature for 90 minutes and then at 210°-220° C for 6 hours. After filtering off the catalyst and stripping off the solvent on a rotary evaporator, 2.4 g of crude 1,10-dicyclooctyl-1,10-diaminodecane are produced.

Provenance & Evidence