HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 39978-68-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-(Adamantan-1-yl)propan-2-amine | HCID 38375 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 39978-68-2 | HCID 38374 | — |
Reaction Steps
β-(1-Adamantyl)-α-methylethylamine (13.3 gm.) was dissolved in 550 ml. anhydrous ether and acidified with HCl gas. The solid was filtered, dried under vacuum at 88°, dissolved in 150 ml. CHCl3, and 850 ml. petroleum ether added to give 15 gm. product, m.p. 295°-7°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04100170 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-b5fb0776596649dca361787739dd370a |
| Source note | uspto-grants-1978_07 |