HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzyl sulfide → C6H5CH2SP(S)Cl2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzyl sulfide | HCID 10867 | — |
| Reactant | Dioctyl sulfide | HCID 75901 | — |
| Reactant | n-C8H17SP(S)Cl2 | HCID 15833785 | — |
| Product | C6H5CH2SP(S)Cl2 | HCID 14939050 | 53% |
Reaction Steps
Following the procedure and employing the reaction temperature and reactants of Example 7 with the exception that 53.5 grams (0.25 mole) of (C6H5CH2)2S were employed as a reactant instead of (n-C8H17)2S, 68 grams (53% yield)of C6H5CH2SP(S)Cl2 was obtained. The product had the following properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04100230 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-05154d3b49bd4f219f5bcec5a8ff4c21 |
| Source note | uspto-grants-1978_07 |