Propane, 1-chloro-3-isocyanato- → HCID 70610686, compound

Participants

Reaction Steps

11.3 gm (38.5 millimols) of N-(p-amino-phenethyl)-N'(m-tolyl)-piperazine, 4.6 gm (38.5 millimols) of 3-chloropropyl-isocyanate and 120 ml of toluene were admixed with each other, accompanied by gentle agitation, and the mixture was allowed to react for 2 hours and was then vacuum-filtered, yielding as the filter cake 90% of theory of N-[p-(3-chloropropyl-ureido)-phenethyl]-N'-(m-tolyl)-piperazine, m.p. 168° C.

Provenance & Evidence