HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Hexan-3-amine | HCID 86062 | — |
| Reactant | 4-Allyl-3-methyl-2,6-dinitrochlorobenzene | HCID 20563841 | — |
| Product | N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline | HCID 54001796 | — |
Reaction Steps
One equivalent of 4-allyl-3-methyl-2,6 -dinitrochlorobenzene is dissolved in three volumes of xylene containing two equivalents of 3-hexylamine. The mixture is refluxed for 5 hours and then poured into water. The organic phase is washed with 5% hydrochloric acid and then water, dried over calcium sulfate, and removed in vacuo to leave the above-named product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101582 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-8e0dea9e00f742baa175cd05a32adff2 |
| Source note | uspto-grants-1978_07 |