HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octadecylamine → HCID 20318442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | HCID 20318402 | HCID 20318402 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20318442 | HCID 20318442 | — |
Reaction Steps
A mixture consisting of 10.6 grams of methyl 3-(5-tert.-butyl-2,3-dimethyl-4-hydroxyphenyl)propionate and 11.9 grams of n-octadecylamine were heated together for 1 hour at 160° to 165° and then at 175° to 180° for 4 hours, the methanol of reaction being removed continuously by distillation. Crystallization from methanol yielded white crystals melting at 85° to 87° (Compound 35).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101550 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-3cb6cc8c226442ca9e5f78d2010aadf3 |
| Source note | uspto-grants-1978_07 |