HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethyl cyclohexylamine → 2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethyl cyclohexylamine | HCID 21609 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-Amino-5-methoxyphenyl)methanol | HCID 13756678 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine | HCID 20319198 | — |
Reaction Steps
2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine was prepared from 2-amino-5-methoxy-benzyl alcohol, thionyl chloride and N-ethyl-cyclohexylamine analogous to Example 1. Proof of structure by IR- and UV-spectra. IR-spectrum (methylenechloride):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101671 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-bea24a1e6b0146f088001926b5e70d92 |
| Source note | uspto-grants-1978_07 |