HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 22750312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22750319 | HCID 22750319 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22750312 | HCID 22750312 | — |
Reaction Steps
From 5.0 g. of 6-[4-(1-piperidinylsulfonyl)phenyl]-1,2-dihydro-2-oxonicotinic acid in 150 ml. of methylene chloride, 2.0 ml. of triethylamine, 1.75 ml. of trimethylsilyl chloride and 2.0 ml. of thionyl chloride, following the procedure of a) above, there is obtained 6-[4-(1-piperidinylsulfonyl)phenyl]-1,2-dihydro-2-oxonicotinyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101661 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-ef745cea94d54fffa3a0a605127f29a6 |
| Source note | uspto-grants-1978_07 |