HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenyl Ether → HCID 20311712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | 1-Acetylpiperidine-4-carbonyl chloride | HCID 100950 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 20311712 | HCID 20311712 | — |
Reaction Steps
By following the manipulative procedure described above in Example 4(a), 32.0 g of 1-acetylisonipecotoyl chloride, [Example 1(b)] are added to a stirring solution of 30.6 g of diphenylether and 45.3 g of aluminum chloride in 100 ml of ethylene dichloride to produce a yellow oil of 1-acetyl- 4-(4-phenoxybenzoyl)piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101663 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-abafdd51b9814c0ab7a0cb9d61f437ee |
| Source note | uspto-grants-1978_07 |