HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 7-[2-(3-acetyloxyoctyl)-4-oxo-3-thiazolidinyl]heptanoate → 7-{2-[2-(Tetrahydro-2H-pyran-2-yl)-ethyl]-4-oxo-3-thiazolidinyl}heptanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 7-[2-(3-acetyloxyoctyl)-4-oxo-3-thiazolidinyl]heptanoate | HCID 20317394 | — |
| Reactant | methyl 7-{2-[2-(tetrahydro-2H-pyran-2-yl)ethyl]-4-oxo-3-thiazolidinyl}heptanoate | HCID 20317400 | — |
| Product | 7-{2-[2-(Tetrahydro-2H-pyran-2-yl)-ethyl]-4-oxo-3-thiazolidinyl}heptanoic Acid | HCID 20317378 | — |
Reaction Steps
This compound is prepared essentially by the method as described in Example 1, Step B, except that the methyl 7-[2-(3-acetyloxyoctyl)-4-oxo-3-thiazolidinyl]heptanoate is replaced by methyl 7-{2-[2-(tetrahydro-2H-pyran-2-yl)ethyl]-4-oxo-3-thiazolidinyl}heptanoate. After chromatographic purification on silica gel, the title compound is obtained as a viscous, pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04102888 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-435c47d162494d9ca7c83cb1a6f26cc4 |
| Source note | uspto-grants-1978_07 |