化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → 1-Amino-6-nitroanthracene-9,10-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | 1,6-Dinitroanthraquinone | HCID 74146 | — |
| 溶媒 | Pentane | HCID 8003 | — |
| 生成物 | 1-Amino-6-nitroanthracene-9,10-dione | HCID 20317509 | 91.5% |
反応手順
310 g of 1,6-dinitroanthraquinone (96%) were reacted 0.5 hours with 340 g of ammonia (molar ratio 20:1; pressure 80 atms) in 1 liter of n-pentane in an autoclave at 150° C.; the reaction mixture obtained was freed from the solvent by distillation. Residue: 269 g of a 91.5% 1-amino-6-nitroanthraquinone (89% of the theoretical yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04102906 |
| 出典データセット | uspto-grants-1978_07 |
| ORD ID | ord-5606c31aadb54e47b3ef2ddf514ad31c |
| 出典メモ | uspto-grants-1978_07 |