5-(1,1-Dimethylheptyl)resorcinol → HCID 11501631, compound

HRID 867127Notes

Reaction equation

HRID 867127 reaction equation
[CH3:1][C:2]([C:10]1[CH:11]=[C:12]([OH:17])[CH:13]=[C:14]([CH:16]=1)[OH:15])([CH3:9])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:18][C:19]1([CH3:34])[CH:24]2[CH2:25][CH:20]1[CH:21]=[CH:22][C:23]2(OC(=O)C)[O:26]C(=O)C>>[CH3:9][C:2]([C:10]1[CH:11]=[C:12]([OH:17])[C:13]([CH:21]2[CH:20]3[CH2:25][CH:24]([C:19]3([CH3:34])[CH3:18])[C:23](=[O:26])[CH2:22]2)=[C:14]([OH:15])[CH:16]=1)([CH3:1])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 918705-(1,1-Dimethylheptyl)resorcinolHCID 20333900HCID 20333900, compound

Product 1

HCID 11501631HCID 11501631, compound

Procedure

Following the same procedure, 1.18 g. of 5-(1,1-dimethylheptyl)resorcinol and 1.19 g. of (+)-6,6-dimethyl-2,2-diacetoxy-3-norpinene were reacted to afford (+)-4-[4-(1,1-dimethylheptyl)-2,6-dihydroxyphenyl]-6,6-dimethyl-2-norpinanone having the identical physical properties as that obtained as described in Example 3.

Sources & evidence

ORD record
ord-c4dcad8f1bfe4a66b05819f5feac7fa7
Source dataset
uspto-grants-1978_07
Patent number
US04102902

Reaction notes

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