HRID867128

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCCCCCC(C)(C)c1cc(O)c2c(c1)OC(C)(C)[C@@H]1CCC(=O)C[C@H]21

HCID86735145

未命名化合物

PRODUCTS

生成物

HCID5284592

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

Evaporation of the solvent from eluates shown by thin layer chromatography to contain a different component afforded 55 mg. of (-)-cis-1-hydroxy-3-(1,1-dimethylheptyl)-6,6-dimethyl-6,6a,7,8,10,10a-hexahydro-9H-dibenzo-[b,d]pyran-9-one. [α]20D - 50° (c = 1.0, CHCl3).

WORKUP

后处理

customEvaporation of the solvent from eluates
customafforded 55 mg