反应详情

m-Trifluoromethyl aniline (32.22 g) in benzene was dissolved in benzene and diketene added slowly with mixing. The reaction mixture was allowed to stand at 25° C. The resulting solid product was recrystallized from ethanol to yield 3'-trifluoromethyl acetoacetanilide.

1. additionwith mixing
2. customto stand at 25° C
3. customThe resulting solid product was recrystallized from ethanol