Ethanolamine → HCID 70624273, compound

HRID 867207Notes

Reaction equation

HRID 867207 reaction equation
[C:1]([C:4]1[CH:5]=[CH:6][C:7]2[C:8](=[O:20])[C:9]3[C:14]([S:15](=[O:19])(=[O:18])[C:16]=2[CH:17]=1)=[CH:13][CH:12]=[CH:11][CH:10]=3)([OH:3])=[O:2].[CH2:21]([CH2:23][NH2:24])[OH:22]>O>[CH2:21]([CH2:23][NH2:24])[OH:22].[C:1]([C:4]1[CH:5]=[CH:6][C:7]2[C:8](=[O:20])[C:9]3[C:14]([S:15](=[O:19])(=[O:18])[C:16]=2[CH:17]=1)=[CH:13][CH:12]=[CH:11][CH:10]=3)([OH:3])=[O:2]

Participants

4

Reactant 2

HCID 700EthanolamineHCID 401183-Carboxy-thioxanthone-10,10-dioxide

Product 1

HCID 70624273HCID 70624273, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To 3-carboxythioxanthone-10,10-dioxide (2.88g) was added a solution of ethanolamine (0.61g) in water (10 ml). The solution was filtered and evaporated to dryness, leaving a residue of 3-carboxythioxanthone-10,10-dioxide ethanolamine salt, m.p. 195° C. with decomposition.

Workup

  1. filtrationThe solution was filtered
  2. customevaporated to dryness

Sources & evidence

ORD record
ord-dc1cc32b358445c3bead1b5456979977
Source dataset
uspto-grants-1978_07
Patent number
US04103015

Reaction notes

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