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HRID867210

反应详情

EQUATION

反应方程式

HRID 867210 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(=O)c1ccsc1
HCID1713652

3-THIENYLGLYOXYLIC ACID

C6H4O3S

结构：CC(C)(C)OC(=O)CON
HCID12919121

tert-Butyl (aminooxy)acetate

C6H13NO3

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)CON=C(C(=O)O)c1ccsc1
HCID54168048

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)(Cl)Cl
溶剂HCID5943

Carbon tetrachloride

CCl4

PROCEDURE

实验过程

Thien-3-ylglyoxylic acid and t-butoxycarbonylmethoxyamine were reacted as described in Preparation 1 to give the title compound, m.p. 102.6°-104.4° (from carbon tetrachloride); λmax (pH6 phosphate buffer) 258 nm (ε 13,700).

WORKUP

后处理

  1. customas described in Preparation 1