HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| Reactant | Acetanilide, 2-chloro-4'-nitro- | HCID 140220 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733006 | — |
Reaction Steps
In a manner similar to that described above in 1a, and using 14.2 parts of N-(3-dimethylaminopropyl)formamide, 20.0 parts of 2-chloro-4'-nitroacetanilide, and 78 parts of isopropyl alcohol there was obtained 27.4 parts of N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid which melted at 195°-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04103092 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-73bd889e4c21417cb275c283151233ab |
| Source note | uspto-grants-1978_07 |